Beamline Alignment Quick Reference: Difference between revisions
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'''1) Select x-ray energy:'''<br /> | '''1) Select x-ray energy:'''<br /> | ||
Calculate scattering angle of Si 111 for desired energy with Bragg law calculator <br /> | Calculate scattering angle of Si 111 for desired energy with Bragg law calculator (or approximate Theta ~ asin(1.977084/E keV) ) <br /> | ||
Drive DCM Theta to the correct Bragg angle for the desired energy, drive undulators approximately to this energy as well <br /> | Drive DCM Theta to the correct Bragg angle for the desired energy, drive undulators approximately to this energy as well <br /> | ||
NOTES:<br /> | NOTES:<br /> | ||
i) If DCM theta looks low for the current energy (~2-4 deg) you may need to re-set user offset (current calibrated theta offset = dial + 8.646deg) <br /> | i) If DCM theta looks low for the current energy (~2-4 deg) you may need to re-set user offset (current calibrated theta offset = dial + 8.646deg) <br /> | ||
ii | ii) Approximate undulator offsets are ~ desired energy +0.1 keV <br /> | ||
Revision as of 14:27, September 8, 2010
Back to X-Ray Microscopy
1) Select x-ray energy:
Calculate scattering angle of Si 111 for desired energy with Bragg law calculator (or approximate Theta ~ asin(1.977084/E keV) )
Drive DCM Theta to the correct Bragg angle for the desired energy, drive undulators approximately to this energy as well
NOTES:
i) If DCM theta looks low for the current energy (~2-4 deg) you may need to re-set user offset (current calibrated theta offset = dial + 8.646deg)
ii) Approximate undulator offsets are ~ desired energy +0.1 keV
2) Scan mirror piezo:
Set slits to
Slit | H Size (mm) | V Size (mm) |
PBS | 0.2 | 2 |
NES | 2 | 2 |
BDA | 2 | - |
scan mirror piezo +/- 1 V. Set mirror piezo to the maximum.
NOTES:
i) mirror piezo feedback should be OFF
ii) CCD shutter should be set to "manual open"
3) Scan DCM 2nd crystal roll:
Set slits to
Slit | H Size (mm) | V Size (mm) |
PBS | 0.2 | 2 |
NES | 0.2 | 2 |
BDA | 2 | - |
scan roll +/- 0.15 mrad. Set roll to maximum - correct for backlash.
NOTES:
i) Correct for backlash by driving to first scan point, then to maximum (e.g. after scan drive relative position -0.15, then drive absolute position to max)
ii) Settling time of at least 1 second is necessary for this scan (this axis is UHV picomotor driven in PID)
4) Scan DCM 2nd crystal pitch:
Set slits to
Slit | H Size (mm) | V Size (mm) |
PBS | 2 | 2 |
NES | 2 | 2 |
BDA | 2 | - |
scan control voltage for DCM piezo tweak +/- 1.5 V. Set piezo to max.
NOTES:
i) if voltage is trending out of range (1V<V<9V), set tweak to 4.5V and scan theta2 motion +/- 0.1mrad
5) Scan Undulators:
Scan upstream and downstream undulators +/- 0.25 keV, drive to max
NOTES:
i) Settling time of at least 1 second is necessary for this scan (possibly more)